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MirayHDCloneProfessionalEdition42rarrar EXCLUSIVE

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MirayHDCloneProfessionalEdition42rarrar · 4.9 Mb A4 Notebook PDF .This invention relates to a process for preparing polycarbonates using bisphenols. More particularly, this invention relates to a continuous process for the preparation of polycarbonates using bisphenols.
Polycarbonates are useful in many applications, particularly in the preparation of molded products. Known processes for the preparation of polycarbonates use phosgene as a source of carbonic acid. Use of phosgene, however, involves safety considerations. And there has been a search for processes for preparing polycarbonates which do not require the use of gaseous phosgene.
Several methods have been developed which do not require use of phosgene. One such method involves the use of an organolithium compound to introduce the terminal hydroxyl group. Another method involves the use of an alkali metal bicarbonate or a primary or secondary amine compound which is bischlorinated or trischlorinated.
Yet another method involves the use of metal salts of bisphenols, such as alkali metal salts, and is reported in U.S. Pat. No. 4,957,957 to Knau et al.
It has been found that the above-noted methods require the use of solvents and catalysts and are carried out in batch processes.
It has now been found that the above-noted difficulties are avoided if a molten mixture comprising bisphenol and carbonate is contacted with an alkylaryl ether. This method is easily carried out continuously in a stirred reactor.Q:

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